Table 1 Crystallographic data for compounds (I-V)

806013

806014

806010

806011

806012

C₅H₅N₂Cl

C₁₂H₁₁N₂O₂Cl

C₁₂H₁₂N₃O₂Cl

C₁₂H₁₀N₂O₂Cl

C₁₂H₁₀N₃Cl

128.56

250.68

265.70

285.12

295.68

Monoclinic

Orthorhombic

Monoclinic

Triclinic

Triclinic

P2₁/c

P2₁2₁2₁

P2₁/c

$\mathit{P}\text{bar}-1$

$\mathit{P}\text{bar}-1$

11.9337 (10)

5.5003 (7)

17.061 (4)

3.7662 (4)

7.0854 (5)

4.6994 (4)

13.3896 (18)

5.3159 (15)

13.1822 (15)

7.3910 (5)

11.2252 (10)

16.314 (2)

13.700 (4)

13.1943 (15)

24.3724 (18)

90

90

90

109.148 (2)

85.938 (1)

112.601 (2)

90

104.642 (10)

92.991 (2)

82.727 (1)

90

90

90

96.214 (2)

86.869 (1)

581.18 (9)

1201.5 (3)

1202.2 (6)

612.49 (12)

1261.54 (15)

4

4

4

2

4

1.469

1.386

1.468

1.546

1.557

0.33 × 0.28 × 0.15

0.51 × 0.11 × 0.06

0.43 × 0.16 × 0.04

0.58 × 0.15 × 0.03

0.47 × 0.08 × 0.05

Colourless

Colourless

Brown

Colourless

Yellow

0.535

0.309

0.315

0.524

0.321

0.71073

0.71073

0.71073

0.71073

0.71073

0.8444/0.9226

0.8577/0.9829

0.8756/0.9869

0.7509/0.9834

0.8647/0.9857

7105

9878

12497

12709

22025

-16, 16; -6, 6;

-8, 8; -16, 20;

-24, 23; -7, 7;

-5, 5; -18, 18;

-9, 9; -9, 8;

-15, 15

-22, 24

-19, 19

-18, 18

-31, 31

1.9–30.0

2.9–32.6

2.5–30.1

1.6–30.0

1.7–27.5

1670

4357

3500

3538

5750

1531

3289

3007

2847

4709

73

157

164

163

441

1.099

0.98

1.12

1.04

0.98

0.033, 0.092

0.046, 0.105

0.089, 0.237

0.038, 0.107

0.054, 0.163