Table 6 Robustness of the proposed method by half factorial design using 10 µg/mL of each of BIL and MNT
Design order | Experimental factorial design | Dependent responses | |||||
|---|---|---|---|---|---|---|---|
Std order | Run order | %MeOH | CAN | pH | Flow rate | Area 1 | Area 2 |
3 | 1 | 91 | 6.5 | 2.8 | 1.2 | 5,25,951 | 4,577,528 |
8 | 2 | 93 | 6.5 | 3.2 | 1.2 | 5,23,287 | 4,48,416 |
2 | 3 | 93 | 5.5 | 2.8 | 1.2 | 5,28,840 | 4,57,504 |
7 | 4 | 91 | 6.5 | 3.2 | 0.8 | 5,30,803 | 4,62,550 |
4 | 5 | 93 | 6.5 | 2.8 | 0.8 | 5,23,246 | 4,56,989 |
1 | 6 | 91 | 5.5 | 2.8 | 0.8 | 5,25,330 | 4,52,036 |
6 | 7 | 93 | 5.5 | 3.2 | 0.8 | 5,33,911 | 4,68,304 |
5 | 8 | 91 | 5.5 | 3.2 | 1.2 | 5,29,164 | 4,47,743 |