Table 2 Recoveries per clean-up material
From: A new LC–MS/MS method for multiple residues/contaminants in bovine meat
Analytes | Added concentration (µg/kg) | Recovery (%) | ||
|---|---|---|---|---|
DSC-MCAX | Bond Elut | Oasis HLB | ||
Clenbuterol | 0.05 | 88.64 | 91.34 | 104.00 |
0.25 | 82.15 | 77.36 | 105.20 | |
0.50 | 92.44 | 84.12 | 102.20 | |
Brombuterol | 0.05 | 71.34 | 80.64 | 75.64 |
0.25 | 69.75 | 85.22 | 92.01 | |
0.50 | 81.32 | 81.34 | 95.34 | |
Mabuterol | 0.05 | 80.52 | 82.15 | 76.00 |
0.25 | 87.24 | 74.22 | 92.00 | |
0.50 | 83.81 | 91.30 | 95.40 | |
Clenpenterol | 0.2 | 104.12 | 71.38 | 87.50 |
0.5 | 101.36 | 78.33 | 93.80 | |
0.75 | 88.32 | 76.91 | 95.47 | |
Isoxsuprin | 0.2 | 71.26 | 75.12 | 88.50 |
0.5 | 77.84 | 77.46 | 106.40 | |
0.75 | 70.20 | 80.20 | 102.00 | |
Cimbuterol | 0.2 | 81.46 | 77.86 | 95.47 |
0.5 | 82.15 | 81.52 | 99.40 | |
0.75 | 91.46 | 80.16 | 94.53 | |
Ractopamine | 0.2 | 74.12 | 81.36 | 96.50 |
0.5 | 84.56 | 115.32 | 104.40 | |
0.75 | 80.26 | 88.12 | 102.93 | |
Salbutamol | 0.5 | 101.46 | 71.36 | 108.00 |
0.75 | 111.36 | 77.22 | 94.93 | |
1.0 | 100.06 | 74.15 | 86.60 | |
Zilpaterol | 0.5 | 77.25 | 80.01 | 81.40 |
0.75 | 81.46 | 84.32 | 98.93 | |
1.0 | 79.32 | 82.56 | 91.10 | |
Terbutaline | 0.5 | 88.36 | 75.36 | 116.20 |
0.75 | 71.32 | 77.88 | 93.20 | |
1.0 | 74.15 | 80.48 | 77.40 | |
Testosterone | 1.0 | 89.32 | 71.22 | 71.50 |
3.0 | 88.36 | 78.36 | 71.66 | |
5.0 | 81.26 | 77.58 | 71.60 | |
Boldenone | 1.0 | 69.22 | 65.15 | 92.0 |
3.0 | 61.14 | 59.36 | 81.34 | |
5.0 | 74.88 | 67.12 | 77.80 | |
Clostebol | 1.0 | 81.36 | 75.14 | 104.0 |
3.0 | 88.32 | 82.88 | 109.34 | |
5.0 | 85.14 | 80.61 | 100.80 | |
Methyltestosterone | 1.0 | 85.26 | 74.15 | 80.0 |
3.0 | 81.34 | 71.33 | 72.67 | |
5.0 | 95.16 | 85.14 | 90.20 | |
Stanozolol | 1.0 | 64.36 | 62.11 | 93.0 |
3.0 | 67.36 | 65.66 | 91.33 | |
5.0 | 60.22 | 71.33 | 89.20 | |
19 nortestosterone | 1.0 | 79.46 | 81.36 | 105.0 |
3.0 | 74.16 | 72.15 | 113.67 | |
5.0 | 88.12 | 77.48 | 104.20 | |
Zeranol | 1.0 | 81.46 | 70.22 | 75.0 |
3.0 | 77.25 | 71.36 | 82.00 | |
5.0 | 92.18 | 81.35 | 71.80 | |
Taleranol | 1.0 | 75.36 | 80.26 | 71.0 |
3.0 | 67.35 | 75.12 | 80.34 | |
5.0 | 61.36 | 71.36 | 89.60 | |
Amoxicillin | 25.0 | 57.46 | 54.36 | 61.89 |
50.0 | 52.11 | 59.64 | 61.28 | |
75.0 | 51.46 | 55.12 | 79.50 | |
Oxacillin | 150.0 | 81.46 | 77.56 | 106.22 |
300.0 | 74.13 | 71.32 | 92.83 | |
450.0 | 77.85 | 71.88 | 94.08 | |
Cloxacallin | 25.0 | 85.14 | 80.12 | 78.96 |
50.0 | 83.22 | 81.36 | 74.94 | |
75.0 | 91.13 | 85.46 | 86.37 | |
Benzylpenicillin | 25.0 | 66.14 | 50.12 | 85.44 |
50.0 | 59.23 | 55.14 | 102.56 | |
75.0 | 56.77 | 51.36 | 95.39 | |
Ampicillin | 25.0 | 65.17 | 70.64 | 75.64 |
50.0 | 61.22 | 74.32 | 82.90 | |
75.0 | 69.22 | 75.12 | 96.00 | |
Ceftioflur | 500.0 | 88.36 | 81.88 | 95.64 |
1000.0 | 81.23 | 82.56 | 92.32 | |
1500.0 | 84.13 | 90.12 | 93.29 | |
Cephalexin | 100.0 | 74.15 | 81.36 | 105.18 |
200.0 | 76.33 | 90.12 | 106.66 | |
300.0 | 81.22 | 88.56 | 96.12 | |
Enrofloxacin | 50.0 | 91.36 | 80.92 | 113.78 |
100.0 | 77.15 | 81.36 | 76.71 | |
150.0 | 81.34 | 90.15 | 82.24 | |
Ciprofloxacin | 50.0 | 108.12 | 95.16 | 81.13 |
100.0 | 113.56 | 103.12 | 83.35 | |
150.0 | 104.18 | 97.22 | 92.81 | |
Oxytetracycline | 50.0 | 81.36 | 77.36 | 79.08 |
100.0 | 97.32 | 77.18 | 77.25 | |
150.0 | 75.14 | 81.36 | 85.56 | |
Sulfachloropyridazine | 50.0 | 78.65 | 88.22 | 107.27 |
100.0 | 77.23 | 90.12 | 82.92 | |
150.0 | 81.56 | 78.15 | 95.12 | |
Sulfadiazine | 50.0 | 88.15 | 101.32 | 96.98 |
100.0 | 96.15 | 108.17 | 74.94 | |
150.0 | 92.11 | 97.36 | 90.61 | |
Sulfadimetoxine | 50.0 | 104.32 | 85.12 | 74.72 |
100.0 | 92.11 | 91.36 | 85.66 | |
150.0 | 93.14 | 90.12 | 94.37 | |
Sulfadimidine | 50.0 | 74.15 | 77.36 | 86.30 |
100.0 | 78.32 | 70.51 | 96.57 | |
150.0 | 77.36 | 72.12 | 99.23 | |
Sulfamethoxazol | 50.0 | 88.35 | 71.36 | 101.26 |
100.0 | 71.22 | 77.15 | 84.19 | |
150.0 | 70.36 | 80.02 | 92.35 | |
Carbofuran | 5.0 | 71.36 | 84.12 | 79.80 |
10.0 | 70.06 | 81.36 | 92.52 | |
15.0 | 75.18 | 90.12 | 96.93 | |
Carbaryl | 25.0 | 82.08 | 71.34 | 86.04 |
50.0 | 71.46 | 75.18 | 102.20 | |
75.0 | 78.54 | 72.36 | 102.97 | |
Parathion | 25.0 | 59.46 | 61.34 | 65.28 |
50.0 | 62.40 | 64.52 | 72.36 | |
75.0 | 69.77 | 64.36 | 79.82 | |
Malathion | 10.0 | 91.48 | 80.54 | 74.51 |
20.0 | 98.22 | 84.38 | 86.9 | |
30.0 | 95.44 | 71.36 | 87.22 | |
Diazinon | 10.0 | 84.56 | 81.56 | 92.14 |
20.0 | 78.13 | 77.46 | 99.65 | |
30.0 | 79.18 | 76.13 | 93.70 | |
Dimethoate | 25.0 | 67.46 | 70.18 | 65.84 |
50.0 | 60.02 | 71.36 | 71.56 | |
75.0 | 62.15 | 72.15 | 79.80 | |
Atrazine | 25.0 | 74.14 | 104.13 | 85.80 |
50.0 | 81.22 | 105.22 | 99.56 | |
75.0 | 76.54 | 89.36 | 92.85 | |
Permethrin | 25.0 | 92.01 | 91.14 | 104.52 |
50.0 | 88.46 | 88.54 | 102.96 | |
75.0 | 88.18 | 89.13 | 104.17 | |
Cypermethrin | 1000.0 | 78.69 | 70.64 | 99.65 |
2000.0 | 74.36 | 77.22 | 92.43 | |
3000.0 | 81.08 | 72.15 | 97.39 | |
Deltamethrin | 15.0 | 92.46 | 70.64 | 84.40 |
30.0 | 103.12 | 70.88 | 92.60 | |
45.0 | 101.46 | 73.63 | 86.93 | |
Coumaphos | 10.0 | 90.60 | 91.46 | 84.90 |
20.0 | 88.60 | 97.12 | 89.30 | |
30.0 | 85.12 | 92.15 | 94.43 | |
Dichlorophos | 25.0 | 101.35 | 88.36 | 95.36 |
50.0 | 95.17 | 81.22 | 95.15 | |
75.0 | 97.36 | 82.15 | 97.49 | |
Chlorpyrifos | 5.0 | 62.08 | 75.22 | 65.6 |
10.0 | 66.13 | 71.36 | 71.15 | |
15.0 | 65.88 | 70.14 | 77.60 | |
Fenvalerate | 12.5 | 69.54 | 64.66 | 61.47 |
25.0 | 61.32 | 59.14 | 81.4 | |
50.0 | 64.12 | 58.36 | 70.36 | |
Zearalenone | 25.0 | 74.36 | 78.34 | 81.84 |
50.0 | 72.15 | 80.12 | 84.36 | |
75.0 | 72.88 | 88.14 | 93.07 | |
Ochratoxin A | 25.0 | 81.56 | 65.14 | 73.84 |
50.0 | 83.12 | 64.22 | 67.15 | |
75.0 | 81.48 | 69.77 | 86.85 | |