- Reaction conditions: (a) first halide (1.1 mmol), 10b (2 mol%), B2pin2 (1.2 mmol), K3PO4 (3.0 mmol), THF (4 mL), RT, 2 h; (b) second chloride (1.0 mmol), 3.0 M aq. K3PO4 (3.0 mmol), RT, 6 h
- aYield of isolated product
- b2 h for the second step
- c4 h for the second step
- d10 h for the second step