Table 1 The matrix of actual and predicted values of particle size from CCRD experimental design
Run no. | Overhead stirring time (min) | Shear rate (rpm) | Shear time (min) | Cycle of homogenizer (cycle) | Particle size (nm) | |
|---|---|---|---|---|---|---|
Actual | Predicted | |||||
1 | 160.00 | 3200.00 | 10.00 | 14.00 | 102.20 | 104.96 |
2 | 200.00 | 2000.00 | 25.00 | 11.00 | 105.20 | 102.73 |
3 | 200.00 | 4400.00 | 25.00 | 11.00 | 81.83 | 83.81 |
4 | 160.00 | 3200.00 | 20.00 | 14.00 | 77.96 | 76.26 |
5 | 160.00 | 3200.00 | 20.00 | 8.00 | 93.45 | 92.32 |
6 | 120.00 | 4400.00 | 25.00 | 17.00 | 92.67 | 94.23 |
7 | 160.00 | 3200.00 | 20.00 | 14.00 | 89.24 | 89.48 |
8 | 240.00 | 3200.00 | 20.00 | 14.00 | 85.87 | 86.07 |
9 | 200.00 | 4400.00 | 15.00 | 17.00 | 90.20 | 88.55 |
10 | 200.00 | 4400.00 | 15.00 | 11.00 | 81.20 | 84.60 |
11 | 200.00 | 2000.00 | 25.00 | 17.00 | 82.18 | 84.26 |
12 | 120.00 | 2000.00 | 15.00 | 17.00 | 75.31 | 74.99 |
13 | 200.00 | 4400.00 | 25.00 | 17.00 | 82.99 | 88.31 |
14 | 80.00 | 3200.00 | 20.00 | 14.00 | 91.94 | 88.50 |
15 | 160.00 | 3200.00 | 30.00 | 14.00 | 82.53 | 83.54 |
16 | 160.00 | 5600.00 | 20.00 | 14.00 | 77.55 | 78.42 |
17 | 160.00 | 3200.00 | 20.00 | 14.00 | 88.90 | 84.68 |
18 | 120.00 | 4400.00 | 15.00 | 17.00 | 75.28 | 77.32 |
19 | 120.00 | 2000.00 | 15.00 | 11.00 | 87.10 | 86.01 |
20 | 200.00 | 2000.00 | 15.00 | 11.00 | 88.36 | 87.27 |
21 | 120.00 | 4400.00 | 25.00 | 11.00 | 88.77 | 87.82 |
22 | 160.00 | 3200.00 | 20.00 | 14.00 | 89.23 | 88.00 |
23 | 200.00 | 2000.00 | 15.00 | 17.00 | 101.67 | 102.04 |
24 | 160.00 | 3200.00 | 20.00 | 20.00 | 89.91 | 87.36 |
25 | 120.00 | 4400.00 | 15.00 | 11.00 | 81.84 | 84.92 |
26 | 160.00 | 800.00 | 20.00 | 14.00 | 84.53 | 84.92 |
27 | 160.00 | 3200.00 | 20.00 | 14.00 | 85.90 | 84.92 |
28 | 120.00 | 2000.00 | 25.00 | 17.00 | 87.52 | 84.92 |
29 | 120.00 | 2000.00 | 25.00 | 11.00 | 82.15 | 84.92 |
30 | 160.00 | 3200.00 | 20.00 | 14.00 | 87.56 | 84.92 |