Analyte | Actual concentration (μg/ml) | Detected concentration (mean ± SD, n = 6) | RSD (%) | RE (%) | |||
---|---|---|---|---|---|---|---|
Interday | Intraday | Interday | Intraday | Interday | Intraday | ||
11-Keto-beta-boswellic acid | 8.0 | 7.90 ± 0.10 | 8.04 ± 0.15 | 1.26 | 1.86 | −1.25 | 0.50 |
25.0 | 24.90 ± 0.60 | 26.43 ± 0.66 | 2.40 | 2.49 | −1.25 | 5.72 | |
100.00 | 99.60 ± 2.88 | 100.35 ± 2.84 | 2.89 | 2.83 | −0.40 | 0.35 | |
3-O-acetyl-11-keto-beta-boswellic acid | 8.0 | 7.96 ± 0.20 | 8.21 ± 0.20 | 2.51 | 2.43 | −0.50 | 2.62 |
25.0 | 25.08 ± 0.32 | 26.50 ± 0.74 | 1.27 | 2.79 | 0.32 | 6.00 | |
100.00 | 99.70 ± 2.84 | 100.61 ± 2.97 | 2.84 | 2.95 | −0.30 | 0.61 | |
3-O-keto-tirucallic acid | 8.0 | 8.09 ± 0.10 | 8.02 ± 0.24 | 1.23 | 2.99 | 1.12 | 0.25 |
25.0 | 25.05 ± 0.66 | 26.61 ± 0.80 | 2.63 | 3.00 | 0.20 | 6.44 | |
100.00 | 97.90 ± 2.96 | 100.94 ± 2.94 | 3.02 | 2.91 | −2.1 | 0.94 | |
3-O-acetyl-alpha-tirucallic acid | 8.0 | 8.03 ± 0.10 | 7.96 ± 0.11 | 1.24 | 1.38 | 0.37 | −0.5 |
25.0 | 25.06 ± 0.13 | 24.89 ± 0.24 | 0.51 | 0.96 | 0.24 | −0.44 | |
100.00 | 100.21 ± 0.70 | 99.83 ± 0.76 | 0.69 | 0.76 | 0.21 | −0.17 | |
3-O-acetyl-beta-tirucallic acid | 8.0 | 7.98 ± 0.16 | 7.92 ± 0.16 | 2.0 | 2.02 | −0.25 | −1.00 |
25.0 | 26.29 ± 0.64 | 25.43 ± 0.61 | 2.43 | 2.39 | 5.16 | 1.72 | |
100.00 | 99.52 ± 2.80 | 100.63 ± 2.52 | 2.81 | 2.50 | −0.48 | 0.63 | |
Alpha-boswellic acid | 8.0 | 7.85 ± 0.07 | 7.82 ± 0.11 | 0.89 | 1.40 | −1.87 | −2.25 |
25.0 | 24.73 ± 0.22 | 25.61 ± 0.66 | 0.88 | 2.57 | −1.08 | 2.44 | |
100.00 | 98.89 ± 0.90 | 100.41 ± 1.67 | 0.91 | 1.66 | −1.11 | 0.41 | |
Beta-boswellic acid | 8.0 | 7.94 ± 0.10 | 7.96 ± 0.22 | 1.25 | 2.76 | −0.75 | −0.5 |
25.0 | 24.88 ± 0.72 | 25.31 ± 0.40 | 2.89 | 1.58 | −0.48 | 1.24 | |
100.00 | 100.13 ± 1.93 | 97.63 ± 2.88 | 1.92 | 2.94 | 0.30 | −2.37 | |
3-O-acetyl-beta-boswellic acid | 8.0 | 8.03 ± 0.18 | 8.09 ± 0.24 | 2.24 | 2.96 | 0.37 | 1.12 |
25.0 | 25.81 ± 0.60 | 25.68 ± 0.62 | 2.32 | 2.41 | 3.24 | 2.72 | |
100.00 | 100.18 ± 2.53 | 99.37 ± 2.69 | 2.52 | 2.70 | 0.18 | −0.63 |