Limit of detection and limit of quantification development procedures for organochlorine pesticides analysis in water and sediment matrices

Table 2 Analytical figures of merit for organochlorine pesticide analysis in previous studies of water matrices

LOD (ng/L)	LOQ (ng/L)	Recovery	Sample size (L)	Reference	Extraction method	Linearity μg/L	Analyses method
0.04–0.17	–	79.5 ± 8.2	2	[28]	SPE¹	–	GC-ECD
5–35	15–106	70–130	1	[15]	SPE¹	–	GC-ECD
0.6–3	–	78–95	1	[19]	SPE¹	–	GC-ECD
0.08–0.16	–	75–87	1	[13]	SPE¹	–	GC-ECD
0.0005–0.015	–	70–103	1	[14]	SPE¹	–	GC-ECD
10–100	–	91–104.	1	[26]	LLE²	–	GC-ECD
0.01–1.03	–	85–105¤¤	-	[10]	LLE²	–	GC-ECD
5.5–20.6	–	71–101	1	[30]	LLE²	–	GC-ECD
1	–	79–96¤¤¤	1	[9]	LLE²	–	GC-ECD
1–3	5–12	81–95	1	[11]	LLE²		GC-MS

* linearity ng/g, ¤ recovery percentage based on Surrogate Standard, ¤¤ recovery for HCH and DDT, ¤¤¤ Internal standard recovery, 1) solid phase extraction, 2) liquid-liquid extraction.

ISSN: 2661-801X