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Table 1 Products, yields, and melting points related to Scheme 3

From: One-pot synthesis of 2-substituted 4H-3,1-benzoxazin-4-one derivatives under mild conditions using iminium cation from cyanuric chloride/dimethylformamide as a cyclizing agent

No.

Product

Yield (%)

mp (T/ oC)

Lit. mp (T/oC)

2a

86

123-124

123-125 [26]

2b

89

236-238

 

2c

78

106-108

 

2d

79

89-91

 

2e

82

261-263

 

2f

89

184-185

184-185 [27, 28]

2g

80

148-149

147-148 [29]

2h

83

167-168

 

2i

86

202-204

203 [27]