1H NMR | 13C NMRa | |||||
---|---|---|---|---|---|---|
Compound | δ(CH3) | δ(NH2)2 | δ(X)n- | δ(CH3) | δ(C(NH2)2) | δ(X)n- |
2 | 2.20a | 7.96; 8.38 | 18.4 | 168.9 | ||
2.10b | 8.39; 8.90 | |||||
4 | 2.18a | 8.03; 8.41 | 8.41 | 18.4 | 168.9 | 171.5 |
2.06b | 9.71 | 8.42 | ||||
7 | 2.16a | 8.04; 8.38 | 18.4 | 168.8 | 173.8 | |
8 | 2.32a | 8.00; 8.40 | 18.6 | 169.0 | ||
2.09b | 8.30; 8.84 |