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Table 2. Optimization of solvent for the synthesis of rilpivirine with better yield
From:
The development of an effective synthetic route of rilpivirine
Solvents
Method
Temperature (°C)
Time
Yield%
Dioxane
A
90
12 h
0
CH
3
CN
A
reflux
69 h
69
NMP
A
90
16 h
75
Dioxane
B
100
30 min
0
CH
3
CN
B
100
60 min
40
NMP
B
100
60 min
43
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