Table 1 Experimental variables for the different extraction methods studied
Extraction method | Variables | Unit | Levels | ||
|---|---|---|---|---|---|
− 1 | 0 | 1 | |||
HAE | Sample/Solvent ratio | – | 0.05 | – | 0.1 |
EtOH/H2O | % | 30 | – | 70 | |
Time | Min | 2 | – | 8 | |
UAE | Sample/Solvent ratio | – | 0.05 | 0.07 | 0.1 |
EtOH/H2O | % | 30 | 50 | 70 | |
Time | Min | 15 | 38 | 60 | |
MAE | Sample/Solvent ratio | – | 0.05 | 0.07 | 0.1 |
EtOH/H2O | % | 30 | 40 | 50 | |
Time | Min | 5 | 15 | 25 | |
Temperature |  °C | 60 | 90 | 120 | |