BMC Chemistry

Table 1 Fe₃O₄@PDA-Pd NPs-catalyzed hydroreduction reaction of p-nitrochlorobenzene

From: Preparation of sub-microspherical Fe₃O₄@PDA-Pd NPs catalyst and application in catalytic hydroreduction reaction of halogenated aromatic nitro compounds to prepare halogenated aromatic amines

Entry	Catalyst	Solvent	Temperature, time	Conversion^a/%	Selectivity (I)^a/%
1	Fe₃O₄@PDA-Pd NPs	EtOH	30 °C, 4 h	>99	95^b
2	Fe₃O₄@PDA-Pd NPs	THF	30 °C, 4 h	81	98
3	Fe₃O₄@PDA-Pd NPs	THF	50 °C, 5 h	> 99	> 99
4	Pd/C	THF	50 °C, 2.5 h	> 99	84^c

^aGC; ^b about 4% N-ethyl-p-chloroaniline in the product; ^c about 13% aniline in the product

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