| a. Proposed DS method (synthetic mixture) | Reference method [39] | ||||||
---|---|---|---|---|---|---|---|---|
Conc. taken (μg/mL) | % Founda | Conc. taken (μg/mL) | % Founda | |||||
FF | GLY | FF | GLY | FF | GLY | FF | GLY | |
Data | 8.4 | 15.75 | 100.08 | 100.12 | 10.0 | 18.0 | 98.24. | 99.58 |
7.2 | 13.5 | 99.48 | 100.82 | 8.4 | 15.0 | 99.42 | 98.35 | |
6 | 11.25 | 99.56 | 100.40 | 7.8 | 12.0 | 100.13 | 101.35 | |
4.8 | 9 | 100.21 | 100.35 | 6.2 | 9.0 | 99.25 | 100.89 | |
3.6 | 6.75 | 100.03 | 99.49 | 4.5 | 6.0 | 100.47 | 99.36 | |
2.4 | 4.5 | 99.99 | 99.18 | 2.9 | 3.0 | 100.34 | 100.21 | |
\({\bar{\text{X}}}\) | Â | 99.89 | 100.06 | Â | 99.92 | 99.96 | ||
± SD | 0.29 | 0.61 | 0.55 | 1.1 | ||||
t-value | 0.32(10.0) | 0.20 (10.0) | Â | |||||
F-value | 3.62 (5.5) | 3.16 (5.5) |
 | b. Proposed DS method (MDI) | Reference method [39] | ||||||
---|---|---|---|---|---|---|---|---|
Conc. taken (μg/mL) | % Founda | Conc. taken (μg/mL) | % Founda | |||||
FF | GLY | FF | GLY | FF | GLY | FF | GLY | |
Data | 8.4 | 15.75 | 100.89 | 100.88 | 10.0 | 18.0 | 99.21 | 100.28 |
7.2 | 13.5 | 99.52 | 100.25 | 8.4 | 15.0 | 98.90 | 99.35 | |
6 | 11.25 | 100.35 | 100.54 | 7.8 | 12.0 | 100.51 | 98.52 | |
4.8 | 9 | 99.87 | 99.35 | 6.2 | 9.0 | 99.54 | 101.35 | |
3.6 | 6.75 | 100.35 | 100.48 | 4.5 | 6.0 | 100.37 | 100.47 | |
2.4 | 4.5 | 100.08 | 99.36 | 2.9 | 3.0 | 98.50 | 98.52 | |
\({\bar{\text{X}}}\) | Â | 100.18 | 100.14 | Â | 99.51 | 99.75 | ||
± SD | 0.47 | 0.67 | 0.33 | 1.14 | ||||
t-value | 1.41 (10.0) | 0.74 (10.0) | Â | |||||
F-value | 3.24 (5.5) | 3.17 (5.5) |