D-H···A | d(D-H)/Å | d(H···A)/Å | d(D···A)/Å | ∠(DHA)/° |
---|---|---|---|---|
Pbtl-V (C-3) | ||||
(a) N1–H1···O4 | 0.88(2) | 1.92(2) | 2.772(5) | 164(5) |
(b) N3–H3···O2′ii | 0.878(19) | 1.91(2) | 2.790(5) | 177(5) |
(c) N1′–H1′···O4′iii | 0.87(2) | 2.00(2) | 2.832(5) | 160(4) |
(d) N3′–H3′···O2ii | 0.903(19) | 1.99(2) | 2.874 (5) | 168(5) |
Pbtl-VI (C-5) | ||||
(a) N1–H1···O4i | 0.887(14) | 2.108(15) | 2.974(2) | 165.2(18) |
(b) N3–H3···O2′ | 0.887(15) | 1.966(15) | 2.838(2) | 167.3(19) |
(c) N1′–H1′···O4 | 0.898(15) | 2.052(16) | 2.936(2) | 168.0(17) |
(d) N3′–H3′···O2v | 0.892(15) | 1.969(16) | 2.852(2) | 170.7(19) |