Sample number | T [°C] | phase | δ [mm/s] | ΔEQ[mm/s] | Hhyp[T] | RA [%] | Elemental analyses [%] | Assignment | ||
---|---|---|---|---|---|---|---|---|---|---|
N | C | H | ||||||||
1a | 25 | LS Fe(III) | −0.17 | 0.85 | – | 100 | 34.4 | 29.8 | 5.5 | [CoIII(en)3][FeIII(CN)6]⋅ 2H2O |
1b | 130 | LS Fe(III) | −0.15 | 0.98 | – | 100 | 36.0 | 31.2 | 5.4 | [CoIII(en)3][FeIII(CN)6]⋅ ½H2O |
2 | 240 | HS Fe(II) | 1.17 | 2.25 | – | 13.0 | 31.3 | 33.2 | 3.9 | [FeII(en)2(μ-NC) CoIII(CN)4] |
HS Fe(II) | 1.31 | 2.53 | – | 11.4 | ||||||
HS Fe(II) | 1.02 | 1.95 | – | 10.0 | ||||||
HS Fe(III) | 0.22 | 0.60 | – | 65.6 | [FeIII(NH2CH2CH3)2(μ-NC)2 CoII(CN)3] | |||||
3 | 300 | HS Fe(II) | 1.14 | 2.49 | – | 18.4 | 26.8 | 31.9 | 3.0 | [FeII(en)2(μ-NC) CoIII(CN)4] |
HS Fe(III) | 0.25 | 0.45 | – | 81.6 | [FeIII(NH2CH2CH3)2(μ-NC)2 CoII(CN)3] | |||||
4 | 350 | HS Fe(III) | 0.26 | 0.43 | – | 55.7 | 19.9 | 22.8 | 2.0 | [FeIII(NH2CH2CH3)2(μ-NC)2 CoII(CN)3] |
HS Fe(III) | 0.46 | 1.22 | – | 44.3 | FeIII[CoII(CN)5] | |||||
5 | 400 | HS Fe(III) | 0.31 | 0.76 | – | 100 | 0 | 0 | 0 | CoFe2O4 (SP) |
6 | 450 | HS Fe(III) | 0.31 | 0.82 | – | 46.8 | 0 | 0 | 0 | CoFe2O4 (SP) |
HS Fe(III) | 0.29 | −0.01 | 42.6 | 53.2 | CoFe2O4 | |||||
7 | 600 | HS Fe(III) | 0.31 | 0.53 | – | 3.4 | 0 | 0 | 0 | CoFe2O4 (SP) |
HS Fe(III) | 0.29 | −0.01 | 48.6 | 79.1 | CoFe2O4 | |||||
HS Fe(III) | 0.37 | −0.05 | 51.4 | 17.5 | CoFe2O4 |