Compound
|
Proposed method
|
Comparison method (35)
|
---|
Amount taken (μg/mL)
|
Amount found (μg/mL)
|
% Found
|
% Found
|
---|
LEV
|
1.0
|
0.9897
|
98.97
|
99.35
|
|
2.0
|
2.0161
|
100.81
|
100.96
|
|
12.0
|
11.8548
|
98.79
|
99.49
|
|
24.0
|
24.0249
|
100.10
| |
|
28.0
|
28.1452
|
100.52
| |
|
36.0
|
36.0484
|
100.13
| |
|
44.0
|
43.8196
|
99.59
| |
± SD
| | |
99.84 ± 0.76
|
99.93 ± 0.89
|
t-test
| | |
0.16 (2.31)
| |
F-test
| | |
1.37 (5.14)
| |
AMB
|
1.0
|
1.0294
|
102.94
|
100.26
|
|
4.0
|
3.9703
|
99.27
|
99.53
|
|
12.0
|
11.9920
|
99.93
|
100.21
|
|
16.0
|
16.0027
|
100.02
| |
|
20.0
|
20.0134
|
100.07
| |
± SD
| | |
100.45 ± 1.43
|
100.00 ± 0.41
|
t-test
| | |
0.51 (2.45)
| |
F-test
| | |
12.31 (19.25)
| |
- N.B. Each result is the average of three separate determinations.
- The figures between parentheses are the tabulated t and F values at P = 0.05 [38].