Position | δH(J in Hz) | δC | HMBC(1H to 13C) | NOSEY |
---|---|---|---|---|
1 | 1.27(1H, m) | 34.9 | 2, 10, 19 | |
1.96(1H, m) | ||||
2 | 2.31(1H, m) | 31.9 | ||
3 | 4.23(1H, d, J=10 Hz) | 74.2 | 2 | |
4 | 90.2 | |||
5 | 4.74(1H, s) | 84.3 | ||
6 | 83.2 | |||
7 | 4.28(1H, s) | 80.4 | 4, 5, 9, 20 | 8 |
8 | 2.56(1H, s) | 45.4 | 6, 7, 9 | 1, 17 |
9 | 72.3 | |||
10 | 1.99(1H, m) | 48.9 | 1, 4, 9 | |
11 | 1.54(1H, m) | 35.5 | ||
12 | 1.76(1H, m) | 35.3 | ||
2.09(1H, m) | ||||
13 | 74.6 | |||
14 | 5.92(1H, s) | 72.2 | 7, 8, 9, 12, 13, 15, 1″ | 7, 8, 16, 17 |
15 | 145.3 | |||
16 | 5.18(1H, s) | 114.5 | 13, 15, 17 | 8, 11, 12, 17 |
5.17(1H, s) | ||||
17 | 1.91(3H, s) | 19.2 | 13, 15, 16 | |
18 | 0.92(3H, d, J=6.56 Hz) | 13.5 | 9, 12 | |
19 | 0.97(3H, d, J=7.12 Hz) | 15.9 | 1, 2, 3 | |
20 | 4.58(1H, d, J=12) | 67.2 | 6, 7, 1´ | |
4.22(1H, d, J=12) | ||||
1´ | 167.5 | |||
2´ | 129.7 | |||
3´7´ | 8.06(2H, d, J=8 Hz) | 130.0 | ||
4´6´ | 7.37(2H, m) | 128.5 | ||
5´ | 7.61(1H, t, J=7.5 Hz), | 133.2 | ||
1″ | 166.4 | |||
2″ | 129.7 | |||
3″7″ | 7.91(2H, d, J=7.5 Hz) | 129.6 | ||
4″6″ | 7.51(2H, t, J=7.5 Hz) | 128.3 | ||
5″ | 7.48(1H, m) | 133.0 |