Selected bonds | Value (Å) | Selected angles | (°) | Selected bonds | Value (Å) | Selected angles | (°) | Selected bonds | Value (Å) | Selected angles | (°) |
---|---|---|---|---|---|---|---|---|---|---|---|
Complex 1 | Complex 2 | Complex 4 | |||||||||
Pb01-O1 | 2.532(2) | O1-Pb01-O2 | 51.55(6) | Pb1-O1 | 2.406(2) | O1-Pb1-O2 | 46.69(7) | Pb1-O1 | 2.407(3) | O1-Pb1-O4 | 120.61(9) |
Pb01-O2 | 2.586(2) | O1-Pb01-O3 | 85.29(6) | Pb1-O2 | 3.019(2) | O1-Pb1-O3 | 120.44(7) | Pb1-O3 | 2.349(2) | O1-Pb1-N1 | 135.72(9) |
Pb01-O3 | 2.518(2) | O1-Pb01-O4 | 134.86(6) | Pb1-O3 | 2.719(2) | O1-Pb1-O4 | 82.29(7) | Pb1-O4 | 2.718(4) | O1-Pb1-N2 | 75.88(7) |
Pb01-O4 | 2.624(2) | O1-Pb01-N1 | 77.61(7) | Pb1-O4 | 2.3469(19) | O1-Pb1-N1 | 134.83(7) | Pb1-N1 | 2.631(3) | O3-Pb1-O4 | 51.45(9) |
Pb01-N1 | 2.481(2) | O1-Pb01-N2 | 121.56(8) | Pb1-N1 | 2.626(2) | O1-Pb1-N2 | 75.57(7) | Pb1-N2 | 2.585(3) | O3-Pb1-N1 | 80.89(10) |
Pb01-N2 | 2.595(2) | O2-Pb01-O3 | 132.41(7) | Pb1-N2 | 2.593(2) | O2-Pb1-O3 | 88.10(6) | O3-Pb1-N2 | 86.18(8) | ||
O2-Pb01-O4 | 152.80(7) | O2-Pb1-O4 | 83.59(6) | O4-Pb1-N1 | 77.42(10) | ||||||
O2-Pb01-N1 | 75.07(7) | O2-Pb1-N1 | 162.85(6) | O4-Pb1-N2 | 126.01(8) | ||||||
O2-Pb01-N2 | 75.97(7) | O2-Pb1-N2 | 122.19(6) | O1-C1-O2 | 125.1(3) | ||||||
O3-Pb01-O4 | 51.14(6) | O3-Pb1-O4 | 51.33(7) | ||||||||
O3-Pb01-N1 | 77.00(7) | O3-Pb1-N1 | 77.62(7) | ||||||||
O3-Pb01-N2 | 123.39(8) | O3-Pb1-N2 | 126.66(6) | ||||||||
O4-Pb01-N1 | 81.02(7) | O4-Pb1-N1 | 80.09(7) | ||||||||
O4-Pb01-N2 | 82.14(7) | O4-Pb1-N2 | 86.66(7) | ||||||||
N1-Pb01-N2 | 64.29(8) | N1-Pb1-N2 | 62.21(7) | ||||||||
Complex 3 | Complex5 | ||||||||||
Pb1-O1 | 2.453(3) | O1-Pb1-O3 | 82.02(10) | Pb1-O1 | 2.749(5) | O1-Pb1-O2 | 50.02(12) | ||||
Pb1-O2i | 2.741(3) | O1-Pb1-O4 | 78.81(10) | Pb1-O2 | 2.335(3) | O1-Pb1-O3 | 119.74(11) | ||||
Pb1-O3 | 2.333(2) | O1-Pb1-N1 | 135.32(11) | Pb1-O3 | 2.633(5) | O1-Pb1-O4 | 82.56(12) | ||||
Pb1-O4 | 2.816(3) | O1-Pb1-N2 | 77.26(11) | Pb1-O4 | 2.824(3) | O1-Pb1-N1 | 79.17(12) | ||||
Pb1-N1 | 2.604(3) | O1-Pb1-O2i | 146.86(10) | Pb1-N1 | 2.608(4) | O1-Pb1-N2 | 120.32(11) | ||||
Pb1-N2 | 2.612(3) | O3-Pb1-O4 | 49.97(9) | Pb1-N2 | 2.577(4) | O1-Pb1-O1i | 63.24(11) | ||||
Pb1 -Pb1i | 3.7020(2) | O3-Pb1-N1 | 75.55(9) | Pb1 -O1 i | 2.909(5) | O2-Pb1-O3 | 87.25(12) | ||||
O3-Pb1-N2 | 86.32(10) | O2-Pb1 -O4 | 83.42(10) | ||||||||
O2i-Pb1-O3 | 102.13(10) | O2-Pb1 -N1 | 79.52(10) | ||||||||
O4-Pb1-N1 | 112.38(10) | O2-Pb1 -N2 | 77.27(12) | ||||||||
O4-Pb1-N2 | 132.48(10) | O1a-Pb1-O2 | 112.45(13) | ||||||||
O2i-Pb1-O4 | 79.23(10) | O3-Pb1 -O4 | 47.69(13) | ||||||||
N1-Pb1-N2 | 63.34(10) | O3-Pb1 -N1 | 139.85(12) | ||||||||
O2i -Pb1-N1 | 76.46(10) | O3-Pb1 -N2 | 76.38(11) | ||||||||
O2i-Pb1-N2 | 135.46(10) | O1-C1-O2 | 121.9(5) | ||||||||
O1a-Pb1-O3 | 140.20(9) | ||||||||||
O4-Pb1 -N1 | 160.44(13) | ||||||||||
O4-Pb1 -N2 | 121.44(12) | ||||||||||
O3-C3-O4 | 125.2(5) | ||||||||||
O1a-Pb1-O4 | 98.61(11) | ||||||||||
N1-Pb1 -N2 | 63.81(14) |