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Table 3 Summary table for Uncertainty Budget for concentration determination in mg kg -1 by classical gravimetry

From: Evaluation of purity with its uncertainty value in high purity lead stick by conventional and electro-gravimetric methods

Sources

X

u std (x)

u std (x) / X

Uc(mg kg-1)

U Ex (mg kg-1); k=2

Precision

1000.883 mg/kg

0.047 mg/kg

0.000047

1.22

2.44

Atomic mass of PbSO4

303.253 g

0.0578 g

0.000191

Balance (Mettler 220 g)

2.015 g

0.00005 g

0.000025

Balance (Saritorious 41 kg)

2012.734 g

0.1345 g

0.000067

Error in buoyancy

2014.745 g

2.0012 g

0.000993

Weight of PbSO4 precipitate (Mettler 220 g)

0.0741 g

0.00005g

0.000675

Balance (Sartorios 41 kg) for stock solution

50.5918 g

0.00005 g

9.883E-07