|
M
r
|
377.80
|
|
Color and habit
|
dark blue, prism
|
|
Crystal system, space group
|
Triclinic, P
|
|
Crystal dimensions/mm3
|
0.12 × 0.08 × 0.06
|
|
a/Å
|
7.4759(9)
|
|
b/Å
|
9.6901(12)
|
|
c/Å
|
11.2469(15)
|
|
α/°
|
108.785(2)
|
|
β/°
|
96.549(3)
|
|
γ/°
|
112.521(2)
|
|
V/Å3
|
685.77(15)
|
|
Z
|
2
|
|
Dcalc/g cm-3
|
1.830
|
|
Temperature/K
|
120(2)
|
|
θrange for data collection/°
|
1.99-26.00
|
|
No. measured reflections
|
6016
|
|
No. independent reflections (Rint)
|
2668 (0.0371)
|
|
No. observed reflections, I ≥ 2σ(I)
|
1714
|
|
No. refined parameters
|
208
|
|
Ra, wRb[I ≥ 2σ(I)]
|
0.0394, 0.0626
|
|
R, wR [all data]
|
0.0671, 0.0669
|
|
Goodness of fit on F2, Sc
|
0.930
|
|
Max., min. electron density/e Å-3
|
1.382, -0.510
|
