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Table 3 Accuracy and precision data for the determination of the studied drugs by the proposed spectrophotometric method

From: Spectrophotometric determination of certain CNS stimulants in dosage forms and spiked human urine via derivatization with 2,4-Dinitrofluorobenzene

Parameter

Intra-day precision

Inter-day precision

 

Conc. taken

(μg/mL)

Conc.

found

(μg/mL)

% Found

Conc.

taken

(μg/mL)

Conc.

found

(μg/mL)

% Found

PPA

4.0

4.03

100.75

4.0

3.97

99.25

 

6.0

5.98

99.67

6.0

5.88

98.00

 

10.0

10.00

100.00

10.0

9.80

98.00

x ̄ ± SD

100.14 ± 0.55

98.42 ± 0.72

%RSD

0.55

0.73

%Er

0.32

0.42

EPH

7.0

6.98

99.71

7.0

7.07

101.00

 

8.0

8.12

101.50

8.0

8.09

101.12

 

10.0

10.02

100.20

9.0

9.15

101.67

x ̄ ± SD

100.47 ± 0.92

101.26 ± 0.36

%RSD

0.91

0.35

%Er

0.52

0.20

PSE

6.0

6.12

102.00*

6. 0

5.96

99.33

 

10.0

10.23

102.30

10.0

10.07

100.70

 

12.0

12.29

102.42

12.0

12.09

100.75

x ̄ ± SD

102.24 ± 0.22

100.26 ± 0.80

%RSD

0.21

0.80

%Er

0.12

0.46

  1. * Each result is the average of three separate determinations.